Chromatographic
Mostrando 1-12 de 2478 artigos, teses e dissertações.
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1. An Eco-Friendly Proposal by Integrating Chromatographic Fingerprinting and Multivariate Control Chart in a Non-Target Analysis to Evaluate Grape Juices from Different Farming Practices
A potential eco-friendly method without organic solvents is presented by integrating a chromatographic fingerprint and multivariate control chart based on Q residuals to differentiate grape juices from different farming practices. The sample preparation was only water dilution, and the mobile phase was water acidified with sulfuric acid, which can be readily
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. METHODS FOR EXTRACTION AND ISOLATION OF AGATHISFLAVONE FROM POINCIANELLA PYRAMIDALIS
Agathisflavone is a natural biflavone with restricted occurrence in plants. This biflavone presents several biological activities and can be important to developing new drugs. Obtaining such a molecule on a large scale for in vivo tests is a challenge. To date, there are no reports regarding its synthesis; thus, it is important to improve and develop methods
Química Nova. Publicado em: 2022
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3. What is new in non-chromatographic flavonoid purification?
Flavonoids are metabolites occurring in all plant tissues and present different biological activities. They occur in a mixture of similar polarity with laborious separation and purification processes, usually furnishing low yields. Semi-preparative chromatographic methods are universally employed procedures for their isolation. This paper discusses the state
Química Nova. Publicado em: 2022
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4. Chromatographic Profiles of Ethyl Acetate Extracts Produced by Bacillus sp. Collected from the Mangroves in the Brazilian Northeast
The genus Bacillus is Gram-positive, anaerobic or aerobic facultative bacteria, often described to be associated with the mangrove rhizosphere. Secondary products of their metabolism, coming from places affected by pollution and environmental stresses, such as mangroves, have been attracting interest from the biotechnological point of view. In view of this s
Journal of the Brazilian Chemical Society. Publicado em: 2022
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5. DITERPENOS ENT-ABIETANOS DE Euphorbia phosphorea (EUPHORBIACEAE)
Phytochemical study of the roots of Euphorbia phosphorea Mart. (Euphorbiaceae) was carried out through chromatographic techniques, resulting in the isolation of a new ent-abietane diterpene named 11β,12β-dihydroxy-ent-abieta-8(14),13(15)-dien-16,12α-olide (1), and of nine known ent-abietane diterpenes jolkinolide A (2), jolkinolide E (3), euphorin H (4),
Química Nova. Publicado em: 2022
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6. Innovative gas chromatographic determination of formaldehyde by miniaturized extraction and on-fiber derivatization, via SPME and SPME Arrow
Formaldehyde (FA) is a carbonyl compound, ubiquitous in the environment and among the most widespread pollutants: it has exhibited toxic properties and is classified as a human carcinogen. FA is released from several sources, both temporary (e.g., combustion processes) and permanent (e.g., building products). This work proposes an innovative fully-automated
Química Nova. Publicado em: 2022
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7. Determinação de etil-glicuronídeo e etil-sulfato em sangue por UPLC-MS/MS: aplicação clínica em vítimas de trauma
We developed a UPLC-MS/MS method for the quantification of the ethanol metabolites ethyl-glucuronide (EtG) and ethyl-sulfate (EtS) in blood samples. Sample preparation was a protein precipitation with acetonitrile 0.1% formic acid containing internal standards (IS) 0.5 µg mL-1 EtG-D5 and EtS-D5. Chromatographic separation was performed in a fluoro-phenyl co
Química Nova. Publicado em: 2022
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8. Errata
Abstract The objective of this work was to associate the use of biofilms to Lippia sidoides (Lippia) and Morinda citrifolia (Noni) essential oils and their respective major constituents in post-harvest quality components. The evaluations in this study were chromatographic analysis the essential oils, fruit mass reduction effect, total soluble solids, peel co
Arq. Bras. Cardiol.. Publicado em: 2021-07
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9. Cardiomiopatia Dilatada: Nova Variante no Gene da Filamina-C
Abstract The objective of this work was to associate the use of biofilms to Lippia sidoides (Lippia) and Morinda citrifolia (Noni) essential oils and their respective major constituents in post-harvest quality components. The evaluations in this study were chromatographic analysis the essential oils, fruit mass reduction effect, total soluble solids, peel co
Arq. Bras. Cardiol.. Publicado em: 2021-07
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10. Implante Percutâneo de Válvula Aórtica Auxiliada pela Oxigenação por Membrana Extracorpórea para Tratamento de Estenose Aórtica com Choque Cardiogênico
Abstract The objective of this work was to associate the use of biofilms to Lippia sidoides (Lippia) and Morinda citrifolia (Noni) essential oils and their respective major constituents in post-harvest quality components. The evaluations in this study were chromatographic analysis the essential oils, fruit mass reduction effect, total soluble solids, peel co
Arq. Bras. Cardiol.. Publicado em: 2021-07
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11. Triagem Familiar no Diagnóstico da Síndrome do QT Curto após Morte Súbita Cardíaca como Primeira Manifestação em Jovens Irmãos
Abstract The objective of this work was to associate the use of biofilms to Lippia sidoides (Lippia) and Morinda citrifolia (Noni) essential oils and their respective major constituents in post-harvest quality components. The evaluations in this study were chromatographic analysis the essential oils, fruit mass reduction effect, total soluble solids, peel co
Arq. Bras. Cardiol.. Publicado em: 2021-07
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12. Nova Mutação no Gene DSP – Um Caso de Cardiomiopatia Arritmogênica com Fenótipo Isolado do Ventrículo Esquerdo e Alto Risco de Morte Súbita
Abstract The objective of this work was to associate the use of biofilms to Lippia sidoides (Lippia) and Morinda citrifolia (Noni) essential oils and their respective major constituents in post-harvest quality components. The evaluations in this study were chromatographic analysis the essential oils, fruit mass reduction effect, total soluble solids, peel co
Arq. Bras. Cardiol.. Publicado em: 2021-07