Extraction Kinetics
Mostrando 1-12 de 116 artigos, teses e dissertações.
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1. In vitro metabolism of copalic and kaurenoic acids in rat and human liver microsomes
Copalic (CA) and kaurenoic (KA) acids are the main diterpenes found in the oleoresin extracted from the copaiba tree (Copaifera sp). This study aimed to characterize the metabolism of CA and KA in rat and human liver microsomes using liquid chromatography with tandem mass spectrometry (LC-MS/MS). The in vitro assays showed deviations from the Michaelian kine
Quím. Nova. Publicado em: 2021-06
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2. Square-Wave Voltammetry Determination of Ciprofloxacin in Pharmaceutical Formulations and Milk Using a Reduced Graphene Oxide Sensor
In this paper, a simple, sensitive and precise electroanalytical method was developed using a chemically-reduced graphene-oxide (CRGO)-modified glassy carbon electrode and square wave voltammetry (SWV) for determination of ciprofloxacin in pharmaceutical formulations (tablets) and milk samples. Advantages of this sensor include a potential displacement of 10
J. Braz. Chem. Soc.. Publicado em: 16/09/2019
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3. POLYPHENOL OXIDASE AND PEROXIDASE ENZYME ASSAYS IN SWEET POTATO CULTIVARS HARVESTED AT DIFFERENT TIMES
RESUMO Ensaios enzimáticos são baseados em metodologias descritas na literatura. Entretanto, a cinética enzimática deve ser ajustada para resultados mais confiáveis. Objetivou-se ajustar os ensaios testando diferentes volumes de extrato de polifenoloxidase (PPO) e peroxidase (POD) e tempos de reação em cultivares de batata-doce colhidas em diferentes
Rev. Caatinga. Publicado em: 18/07/2019
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4. KINETICS OF THE BIODEGRADATION OF MONOAROMATICS BY Pseudomonas aeruginosa
ABSTRACT Water contamination by monoaromatic compounds has risen throughout time, which leads to the necessity of developing new water treatment technology, capable of minimizing their negative effect on the environment. In this context, biological processes present themselves as a solution to the processes of extraction. Bioremediation makes use of microbia
Braz. J. Chem. Eng.. Publicado em: 15/07/2019
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5. Drying and extraction of astaxanthin from pink shrimp waste (Farfantepenaeus subtilis ): the applicability of spouted beds
Abstract In this study, the spouted bed drying technique was used to obtain powder from shrimp wastes, with high quality for subsequent extraction of astaxanthin using vegetable oil, as alternative to organic solvents. Shrimp waste paste was dried in three inlet air temperatures (70, 80 and 90 °C), and air velocity used in the experiments was 100% over min
Food Sci. Technol. Publicado em: 30/07/2018
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6. Development of a Method Based on DLLME and UFLC-DAD for the Determination of Antibiotics in Honey Samples and the Study of Their Degradation Kinetics
In this work, a method was developed, based on dispersive liquid-liquid microextraction (DLLME) and analysis by ultra-fast liquid chromatography coupled to diode array detector (UFLC-DAD), to simultaneously determine ten antibiotics of two different classes in honey, as well as to evaluate their degradation kinetics in this matrix. The extraction was optimiz
J. Braz. Chem. Soc.. Publicado em: 2018-07
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7. Surface Imprinting of Silica Gel by Methyldopa and Its Application in the Solid Phase Extraction Procedure
An imprinted amino-functionalized silica gel material was prepared by surface molecular imprinting technique combined with a sol-gel process on the supporter of activated silica gel and used as a solid-phase extraction for the extraction and determination of methyldopa (MTD). Non-imprinted silica adsorbent was synthesized without the addition of MTD using th
J. Braz. Chem. Soc.. Publicado em: 2018-02
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8. Leaching kinetics of ulexite ore in aqueous medium at different CO 2 partial pressures
Abstract This manuscript presents a study regarding the leaching kinetics of ulexite (Na2O.2CaO.5B2O3.16H2O) under different CO2 partial pressures in aqueous media. The effects of the reaction temperature, particle size, CO2 partial pressure, solid-liquid ratio, and agitation speed were investigated in the boron extraction from the ore. As a result of the ex
Braz. J. Chem. Eng.. Publicado em: 2018-01
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9. THEORETICAL RESEARCH ON THE MULTI-CHANNEL REACTION MECHANISM AND KINETICS OF HNCS WITH OH-
We presented a theoretical study on the detailed reaction mechanism and kinetics of the HNCS molecule with the OH-. The barrierless minimum energy path and the most favorable entrance channel have been determined by study the thermodynamic and kinetic characters of the channel with low energy barrier. The B3LYP/6-311++G** method was employed for all the geom
Quím. Nova. Publicado em: 2017-10
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10. PEROXIDASE FROM SOYBEAN MEAL: OBTENTION, PURIFICATION AND APPLICATION IN REDUCTION OF DEOXYNIVALENOL LEVELS
This study established the conditions for the extraction of the enzyme peroxidase (PO) from soybean meal (SBM). An experimental design methodology was carried out in order to evaluate the effects of stirring rate time, pH and extracting solvent volume on the enzyme extraction. By using 5 g SBM and 50 mL phosphate buffer 10 mmol L-1 pH 4.7, 60 min stirring ra
Quím. Nova. Publicado em: 2017-09
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11. Influence of microwave irradiation on kinetics and thermodynamics of extraction of flavonoids from Phyllanthus emblica
Abstract-The effects of solvent-to-feed (S) and temperature (T) on the kinetics and thermodynamics of the microwave assisted extraction (MAE) of flavonoids from dried fruits of Phyllanthus emblica using water as solvent have been studied. The flavonoid concentration - time data was analyzed using second order and diffusion models. Both the temperature and so
Braz. J. Chem. Eng.. Publicado em: 2017-07
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12. KINETICS OF ULTRASOUND ASSISTED EXTRACTION OF WEDELOLACTONE FROM Eclipta alba
Abstract Ultrasound assisted extraction of wedelolactone, a major coumestan present in Eclipta alba, is investigated in the present work.Various process parameters such as type of solvent, power, solvent to solid ratio and extraction temperature, which affect the extraction yield, are optimized. In the ultrasound-assisted extraction with final optimized cond
Braz. J. Chem. Eng.. Publicado em: 2016-12