Gf Aas
Mostrando 1-12 de 85 artigos, teses e dissertações.
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1. Simple Spectrophotometric Determination of Iron in Diesel Oil after Sample Preparation Employing Extraction Induced by Emulsion Breaking
This work reports the development of a simple and fast method for the spectrophotometric determination of Fe in diesel oil using the classic reaction with 1,10-phenanthroline after its extraction induced by emulsion breaking (EIEB). The extraction parameters of EIEB were optimized (concentration of HNO3 and Triton X-100® in the emulsifying solution) as well
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Dispersive Solid-Phase Extraction Using 3-Mercaptopropyltrimethoxysilane Functionalized Magnetic MWCNT-Based Nanocomposite for Selective and Efficient Preconcentration of Pb2+ with FAAS Determination
A novel nanocomposite based on magnetic multiwalled carbon nanotubes coated with SiO2 and functionalized with 3-mercaptopropyltrimethoxysilane (3-MPTMS) was prepared for the efficient extraction and quantification of lead ions from water samples. The adsorption capacity of this adsorbent could reach 1.995 mg g-1 Pb2+ in an equilibrium time of 30 min. Under o
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. Development of a Methodology Based on Extraction Induced by Emulsion Breaking for Copper Determination in Gasohol by Graphite Furnace Atomic Absorption Spectrometry
The development of a method based on extraction induced by emulsion breaking (EIEB) aiming copper determination in gasohol using graphite furnace atomic absorption spectrometry (GF AAS) is reported. Emulsification of the gasohol samples was carried out using nitric acid solution, (1,1,3,3-tetramethylbutyl)phenyl-polyethylene glycol surfactant (Triton X-114),
J. Braz. Chem. Soc.. Publicado em: 2021-02
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4. Determination of Copper and Cadmium in Petroleum Produced Formation Water by Electrothermal Atomic Absorption Spectrometry after Cloud Point Extraction
Cloud point extraction (CPE) in association with graphite furnace atomic absorption spectrometry (GF AAS) was proposed for preconcentration and quantification of trace amounts of copper and cadmium in samples of saline produced formation water from petroleum exploration. The procedure was based on the formation of hydrophobic complexes of the analytes with 1
J. Braz. Chem. Soc.. Publicado em: 2020-06
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5. Evaluation of metals in tomato sauces stored in different types of packaging
Abstract There is a growing concern about health and food safety when it comes to processed food. In the present study, it has been hypothesized that tomato sauces contain high amounts of metals possibly leached from packaging. Concentrations of As, Cd, Pb, Cr, Ni, Sn and Sb were determined by ICP-MS in tomato sauces stored in metallic, plastic, cellulosic
Food Sci. Technol. Publicado em: 26/07/2018
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6. CORRELAÇÕES GEOQUÍMICAS ENTRE AMOSTRAS DE PETRÓLEO DA BACIA POTIGUAR E DEFINIÇÃO DE SUAS POSSÍVEIS ROCHAS GERADORAS
Eight petroleum samples from Potiguar Basin were submitted for determination of saturated biomarkers by gas chromatography (fingerprint), liquid chromatography (saturates, aromatics, resins and asphaltenes), gas chromatography-mass spectrometry (GC-MS), nickel and vanadium by high resolution continuum source graphite furnace atomic absorption spectrometry (H
Quím. Nova. Publicado em: 2018-04
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7. Alkaline Solubilization of Chicken Tissues Monitored by Raman Spectroscopy Followed by Pb Determination by GF AAS
This paper proposes a method for chicken tissues preparation using tetramethylammonium hydroxide (TMAH) for Pb determination by graphite furnace atomic absorption spectrometry employing multivariate approaches. Combining Raman spectroscopy with scanning electron microscopy coupled to energy-dispersive X-ray spectroscopy to monitor the solubilization process
J. Braz. Chem. Soc.. Publicado em: 2018-02
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8. IN VITRO Cr(VI) SPECIATION IN SYNTHETIC SALIVA AFTER RELEASING FROM ORTHODONTIC BRACKETS USING SILICA-APTES SEPARATION AND GF AAS DETERMINATION
A method for Cr(VI) speciation in synthetic saliva after releasing from orthodontic brackets, using silica nanoparticles organofunctionalized with (3-aminopropyl)triethoxysilane (APTES) for Cr(III)/Cr(VI) separation and GF AAS determination is proposed. Under the optimized conditions, Cr(VI) speciation was performed using 150 mg of silica organofunctionalize
Quím. Nova. Publicado em: 2016-09
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9. Feasibility of Using AAS for the Characterization of a Tuna Fish Candidate Reference Material for Total Hg and Methyl-Hg Measurement
This work describes the evaluation of several parameters for preparing a tuna fish candidate reference material (RM) in order to measure its total Hg and methyl-Hg mass fractions by cold vapor atomic absorption spectrometry (CV-AAS) and solid sampling graphite furnace atomic absorption spectrometry (SS-GF AAS). Best results were acquired after extraction wit
J. Braz. Chem. Soc.. Publicado em: 2016-04
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10. Fast Determination of Iron and Zinc in Hair and Human Serum Samples After Alkaline Solubilization by GF AAS
Methods for the development and validation for determination of iron and zinc in human serum and hair samples by graphite furnace atomic absorption spectrometry (GF AAS) were performed. Solubilization was immediate by manual agitation in both samples with a 10 mL volume sample plus deionized water. Optimum pyrolysis and atomization temperatures were obtained
J. Braz. Chem. Soc.. Publicado em: 2016-01
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11. Determination of Essential, Non-Essential, and Potentially Toxic Elements in Graviola (Annona muricata L.) Pulp by ICP OES and GF AAS
The determination of essential (B, Ca, Co, Cu, Cr, Fe, K, Li, Mg, Mn, P, S, Se, Si, V, and Zn), non-essential (Al, Ba, Sn, Sr, and Ti), and potentially toxic (As, Cd, and Pb) elements in graviola pulp by inductively coupled plasma optical emission spectrometry (ICP OES) and graphite furnace atomic absorption spectrometry (GF AAS) is proposed. Samples were di
J. Braz. Chem. Soc.. Publicado em: 2015-10
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12. Chemical Speciation of Iron in Different Varieties of Beans (Phaseolus vulgaris L.): Cooking Effects
Beans are considered a source of iron (Fe), and hence have considerable contribution in cases of Fe deficiency. Beans also contain certain anti-nutritional constituents, which are imperative to the cooking of beans. The nutritional value of beans depends on the bioavailability, which can be affected by cooking. Studies about heating effects in distribution o
J. Braz. Chem. Soc.. Publicado em: 2015-10