Purification Techniques
Mostrando 1-12 de 273 artigos, teses e dissertações.
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1. What is new in non-chromatographic flavonoid purification?
Flavonoids are metabolites occurring in all plant tissues and present different biological activities. They occur in a mixture of similar polarity with laborious separation and purification processes, usually furnishing low yields. Semi-preparative chromatographic methods are universally employed procedures for their isolation. This paper discusses the state
Química Nova. Publicado em: 2022
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2. METHODS FOR EXTRACTION AND ISOLATION OF AGATHISFLAVONE FROM POINCIANELLA PYRAMIDALIS
Agathisflavone is a natural biflavone with restricted occurrence in plants. This biflavone presents several biological activities and can be important to developing new drugs. Obtaining such a molecule on a large scale for in vivo tests is a challenge. To date, there are no reports regarding its synthesis; thus, it is important to improve and develop methods
Química Nova. Publicado em: 2022
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3. DESVENDANDO UM CASO: QUANDO ESTUDANTES SE TORNAM PERSONAGENS DE UMA HISTÓRIA NA DISCIPLINA DE QUÍMICA ORGÂNICA EXPERIMENTAL
Being part of the Pharmacy course curriculum, Organic Chemistry emphasizes the fundamentals of Organic Synthesis, reaction mechanisms, as well as the methods for separation, purification and identification of organic compounds. However, students do not always realize the direct association between this knowledge and their future working field. In an effort t
Química Nova. Publicado em: 2022
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4. Brazilian Mineral Clays: Classification, Acid Activation and Application as Catalysts for Methyl Esterification Reactions
In this study, three raw Brazilian clays from João Pessoa, Paraíba State (Aço AP, AVL and Verde Lodo) were characterized before and after purification and acid activation. Several instrumental techniques were used, and the raw clays were classified as dioctahedral smectites with different compositions, where the AVL sample had the highest content of montm
J. Braz. Chem. Soc.. Publicado em: 2021-01
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5. Improvement of Mycobacterium tuberculosis detection in sputum using DNA extracted by sonication
Abstract Tuberculosis (TB) is one of the infectious diseases with high mortality in the world. DNA amplification techniques have been used to overcome barriers to the diagnosis of this disease. However, the success of these methodologies is highly dependent on the DNA obtained from the sample. This study was carried out to verify whether the DNA extracted by
Braz J Infect Dis. Publicado em: 2020-10
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6. AVALIAÇÃO DE NANOTUBOS DE CARBONO FUNCIONALIZADOS VISANDO O DESENVOLVIMENTO DE MÉTODOS DE PRÉ-CONCENTRAÇÃO DE ÍONS METÁLICOS E DETERMINAÇÃO POR TÉCNICAS ESPECTROMÉTRICAS E ELETROANALÍTICAS
This review focuses on the use of functionalized carbon nanotubes (CNTs) on the development of preconcentration methods with substantial contributions on selectivity and sensitivity for metal ions determination. CNTs have been usually employed in the development of preconcentration/speciation coupled to spectroanalytical techniques for ions determination at
Quím. Nova. Publicado em: 2020-09
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7. Errata
ABSTRACT Oleuropein is one of the most abundant phenolic compounds present in olive leaves, and many studies have shown that this compound has important biological properties (anti-inflammatory, anti-atherogenic, anticancer, antimicrobial and antiviral) and that is why it has been gaining prominence in research. Oleuropein can be extracted from different sou
Arq. Bras. Cardiol.. Publicado em: 2020-08
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8. Oleuropein: Methods for extraction, purifying and applying
ABSTRACT Oleuropein is one of the most abundant phenolic compounds present in olive leaves, and many studies have shown that this compound has important biological properties (anti-inflammatory, anti-atherogenic, anticancer, antimicrobial and antiviral) and that is why it has been gaining prominence in research. Oleuropein can be extracted from different sou
Rev. Ceres. Publicado em: 2020-08
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9. Cell-Based Therapies for Myocardial Regeneration in Heart Failure: 20 Years of Debate
ABSTRACT Oleuropein is one of the most abundant phenolic compounds present in olive leaves, and many studies have shown that this compound has important biological properties (anti-inflammatory, anti-atherogenic, anticancer, antimicrobial and antiviral) and that is why it has been gaining prominence in research. Oleuropein can be extracted from different sou
Braz. J. Cardiovasc. Surg.. Publicado em: 2020-08
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10. Activated carbon loaded with manganese and iron for glyphosate adsorption: Kinetics, isotherms and thermodynamic studies
Resumo Carvão ativado granular foi impregnado com 1% de ferro e 0,5% de manganês (m/m) para remoção de glifosato em soluções aquosas. O adsorvente foi caracterizado por microscopia eletrônica de varredura, espectroscopia de energia dispersiva, técnicas de adsorção de nitrogênio e análises de potencial zeta. Estudos em batelada foram realizados pa
Rev. Ambient. Água. Publicado em: 25/11/2019
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11. Pentacyclic triterpenes and other constituents in propolis extract from Melipona beecheii collected in Yucatan, México
ABSTRACT Thirteen pentacyclic triterpenes, methyl 3-oxours-12-en-23-oate, marsformosanone, taraxerone, β-amyrenone, α-amyrenone, lupenone, 24-methylencycloartan-3-one, moretenol acetate, β-amyrin acetate, germanicol acetate, 24-methylencycloartanyl acetate, β-amyrin, and α-amyrin were identified in a chloroform-methanol propolis extract from Melipona be
Rev. bras. farmacogn.. Publicado em: 26/08/2019
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12. Produção e purificação integrada de protease fibrinolítica de Mucor subtilissimus UCP 1262
RESUMO As enzimas fibrinolíticas podem ser obtidas de micro-organismos por meio de processos fermentativos. O presente trabalho teve como objetivo avaliar a produção e extração integrada da protease fibrinolítica de Mucor subtilissimus UCP 1262 usando sistema de duas fases aquosas (SDFA). O processo integrado foi realizado para avaliar a produção, pa
Arq. Bras. Med. Vet. Zootec.. Publicado em: 06/06/2019