Small Angle Scattering
Mostrando 1-12 de 187 artigos, teses e dissertações.
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1. Hybrid Hydrogels Based on Polyethylene Glycol Bioconjugated with Silylated-Amyloidogenic Peptides
Hybrid-peptide hydrogel arrangements are a promising alternative to obtaining biocompatible structures at the nanoscopic scale. In this work, a new class of hybrid hydrogels was obtained through the sol-gel process based on the reaction between an amyloid-like octapeptide sequence [RF]4 (where R = arginine and F = phenylalanine) covalently bonded with glycin
J. Braz. Chem. Soc.. Publicado em: 2020-11
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2. Influence of the Capping Agent PVP of the Outer Layer of Pd Nanocubes Surface on the Catalytic Hydrogenation of Unsaturated C−C Bonds
The excess of capping agents used during the synthesis of nanoparticles is usually removed by solvent washing. The influence of the amount of polyvinylpyrrolidone (PVP) capping agent in the catalytic activity of palladium nanocubes was evaluated, after different numbers of washing cycles in the purification step performed after the syntheses of the nanoparti
J. Braz. Chem. Soc.. Publicado em: 2020-05
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3. Scientific Literature of Small-Angle X-Ray and Neutron Scattering Applied to the Characterization of Materials at the Nanometer Scale
The SAXS and SANS techniques are widely applied to the structural characterization of materials at the nanometer scale. We here report quantitative analyses of the published literature related to these techniques and to relevant features of the International SAS Conferences. A total number of 42,048 articles related to SAXS and SANS were retrieved. The annua
Mat. Res.. Publicado em: 25/11/2019
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4. Acid Hydrolysis of Regular Corn Starch under External Electric Field
The main objective of the present work is the investigation of a new method for starch hydrolysis. For this, we proposed the acid hydrolysis under the action of an external electric field, able to develop a faster reaction than the conventional one. Corn starch with 18% amylose was subjected to a fixed voltage, varying the external electric field application
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
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5. Analysis of Molecular Changes Induced By Mineral Trioxide Aggregate On sPLA2
Resumo O objetivo deste estudo foi analisar os efeitos do MTA na estrutura e atividade enzimática da sPLA2 a fim de fornecer subsídios para melhoria na formulação do produto. O MTA em pó foi incubado por 60 min na presença de sPLA2 e analisado por cromatografia, espectroscopia de massa por eletropulverização (ESI-MS) e espalhamento de raios-X de baix
Braz. Dent. J.. Publicado em: 07/10/2019
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6. Insights on Structuration of Peroxotungstic Acid in Aqueous Media
Recent studies on tungsten oxide preparation are mainly motivated by its applications in smart windows, energy harvesting and, recently, in cancer therapy. Peroxotungstic acid (PTA) is an important precursor to obtain tungsten oxide in an environmentally-friendly way, through the colloidal synthesis in aqueous media. Despite giving chemically pure products,
J. Braz. Chem. Soc.. Publicado em: 2019-04
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7. Effects of artepillin C on model membranes displaying liquid immiscibility
It has been hypothesized that the therapeutic effects of artepillin C, a natural compound derived from Brazilian green propolis, are likely related to its partition in the lipid bilayer component of biological membranes. To test this hypothesis, we investigated the effects of the major compound of green propolis, artepillin C, on model membranes (small and g
Braz J Med Biol Res. Publicado em: 25/03/2019
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8. Jaburetox: update on a urease-derived peptide
Abstract Urease from Canavalia ensiformis seeds was the first enzyme ever to be crystallized, in 1926. These proteins, found in plants, bacteria and fungi, present different biological properties including catalytic hydrolysis of urea, and also enzyme-independent activities, such as induction of exocytosis, pro-inflammatory effects, neurotoxicity, antifungal
J. Venom. Anim. Toxins incl. Trop. Dis. Publicado em: 08/02/2018
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9. Organic cocoa extract -loaded surfactant-based systems intended to skin bioadhesion
ABSTRACT This study was to develop, characterize, and evaluate the physical-chemical stability, in vitro antioxidant activity and in vitro safety profile of liquid crystalline systems (LCS) and microemulsions (MEs) with and without organic cocoa (OC) extract. LCS stabilized by surfactant polyoxyethylene 20 cetyl ether, containing water and oleic acid were st
Braz. J. Pharm. Sci.. Publicado em: 26/10/2017
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10. Nanostructured Antigen-Responsive Hydrogels Based on Peptides for Leishmaniasis Detection
Hydrogels based on peptide nanostructures are biological entities that can be applied in a wide range of applications, such as scaffolds for tissue engineering, drug delivery, and biosensors. The aim of this research was to study peptide hydrogels based on N-(9-fluorenylmethoxycarbonyl)-L, L-diphenylalanine (Fmoc-FF) in two different media: water and phospha
J. Braz. Chem. Soc.. Publicado em: 2017-09
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11. Development and Characterization of Vitamin A-Loaded Solid Lipid Nanoparticles for Topical Application
Vitamin A and its esters are commonly found in topical applications because of their advantageous properties, however, have the drawback that are highly sensitive to ultraviolet radiation. The aim of this work was to develop and characterize a novel formulation of solid lipid nanoparticles suitable for topical applications in order to protect vitamin A from
J. Braz. Chem. Soc.. Publicado em: 2017-07
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12. SÍNTESE E PROPRIEDADES DE SÍLICAS HÍBRIDAS CONTENDO SURFACTANTES CETILTRIALQUILAMÔNIO
This work presents the synthesis of silicas containing cetyltrialkylammoniun surfactants in their mesopores. Initially, the aqueous dispersions of these surfactants were characterized by small-angle X-ray scattering (SAXS). The hybrid silicas obtained from these dispersions were evaluated by X-ray diffractometry (XRD) and nitrogen physisorption. The XRD show
Quím. Nova. Publicado em: 2016-04